Yue Yu*
FDMP-Fluid Dynamics & Materials Processing, Vol.19, No.10, pp. 2681-2694, 2023, DOI:10.32604/fdmp.2023.028250
- 25 June 2023
Abstract A triethylenetetramine epoxy mixture was synthesized through the reaction of a low-molecular-weight liquid epoxy resin with triethylenetetramine (TETA). Then triethyltetramine (TETA) was injected dropwise into a propylene glycol methyl ether (PM) solution for chain extension reaction. A hydrophilic and flexible polyether segment was introduced into the hardener molecule. The effects of TETA/DGEPG, reaction temperature and reaction time on the epoxy conversion of polyethylene glycol diglycidyl ether (DGEPG) were studied. In addition, several alternate strategies to add epoxy resin to the high-speed dispersion machine and synthesize MEA DGEBA adduct (without catalyst and with bisphenol A diglycidyl More >