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  • Open Access

    ARTICLE

    Effect of Drying Methods on the Morphology and Electrochemical Properties of Cellulose Gel Polymer Electrolytes for Lithium-Ion Batteries

    Jiling Song1, Hua Wang2,*, Jianbing Guo1, Minghua Lin2, Bin Zheng2,*, Jiqiang Wu3,*

    Journal of Polymer Materials, Vol.42, No.4, pp. 1143-1157, 2025, DOI:10.32604/jpm.2025.073414 - 26 December 2025

    Abstract The pursuit of safer energy storage systems is driving the development of advanced electrolytes for lithium-ion batteries. Traditional liquid electrolytes pose flammability risks, while solid-state alternatives often suffer from low ionic conductivity. Gel polymer electrolytes (GPEs) emerge as a promising compromise, combining the safety of solids with the ionic conductivity of liquids. Cellulose, an abundant and eco-friendly polymer, presents an ideal base material for sustainable GPEs due to its biocompatibility and mechanical strength. This study systematically investigates how drying methods affect cellulose-based GPEs. Cellulose hydrogels were synthesized through dissolution-crosslinking and processed using vacuum drying (VD),… More >

  • Open Access

    ARTICLE

    Influence of Honey on Structural, Morphology and Thermal Behavior of Zein-Based Polymer Systems

    Nurrul Asyiqin K. Shamsuri1, Shujahadeen B. Aziz2, Siti Nadiah Halim3, Hashlina Rusdi4, Mohd Fakhrul Zamani Kadir1,5,*

    Journal of Polymer Materials, Vol.42, No.4, pp. 1111-1123, 2025, DOI:10.32604/jpm.2025.070939 - 26 December 2025

    Abstract This study investigates the effects of honey concentration on the crystallinity, morphology, and thermal behavior of zein-based polymer systems, aiming to assess honey’s role as a natural plasticizer. Fourier transform infrared spectroscopy (FTIR) analysis confirmed the presence of strong intermolecular interactions and hydrogen bonding between zein and honey, indicating good miscibility. X-ray diffraction (XRD) patterns revealed a significant reduction in crystallinity with increasing honey concentration up to 25 wt.%, with the ZH5 (75 wt.% zein-25 wt.% honey) sample exhibiting the smallest crystallite size (4.23 nm), suggesting enhanced amorphous character suitable for ionic mobility. Field emission… More >

  • Open Access

    ARTICLE

    Morphological study of bulk sample averse to thin films for a quaternary glassy alloy system

    P. Kaushika,*, A. Devib, H. Singha

    Chalcogenide Letters, Vol.22, No.3, pp. 197-204, 2025, DOI:10.15251/CL.2025.223.197

    Abstract The structural properties of bulk as well as thin films of nanostructured Bi1Te15Se84-x Pbx (0 ≤ x ≤ 8) glassy alloys has been studied in this paper. Conventional melt quenching method is employed to prepare the samples of Bi1Te15Se84-x Pbx (0 ≤ x ≤ 8) alloys. Thin films with thickness of approximately 158nm of the obtained bulk compositions were deposited on dry cleaned glass substrates by thermal evaporation technique. The structural characterization was carried out using XRD and SEM. Energy dispersive X-ray spectroscopy (EDX) indicates that samples are nearly stoichiometric. X-ray diffraction patterns indicate that they are More >

  • Open Access

    ARTICLE

    The effect of aluminum doping on nanostructured CdS: optical, structural and sensing characterization

    H. R. Shakira, O. A. Chichanb, M. S. Sadac,*, S. A. Husseind, S. S. Chiade, N. F. Habubif, Y. H. Kadhimg, M. Jadanh,i

    Chalcogenide Letters, Vol.22, No.1, pp. 77-89, 2025, DOI:10.15251/CL.2025.221.77

    Abstract CdS, and CdS: Al were grown onto glass bases via Chemical spray pyrolysis (CSP). XRD analysis of CdS films indicates a polycrystalline hexagonal structure with a predominant orientation of the (101) plane. The strain decreased from 28.55 to 25.66, and the grain size of undoped CdS films was around (13.51–12.14) nm as Al content rose. According to the results of AFM, CdS, CdS:2% Al, and CdS:4% Al all exhibit smooth surfaces with decreasing particle size in the range of (78.46), (69.75), and (42.20) nm, respectively. The root-mean-square roughness values for CdS and CdS:4% Al were… More >

  • Open Access

    ARTICLE

    The importance of CdS and ZnO-NPs in study anti-microbial activity prepared by laser ablation and simple chemical method

    H. A. Ahmed, M. Y. Ali, S. S. Hamood, A. N. Abd*

    Chalcogenide Letters, Vol.22, No.1, pp. 11-22, 2025, DOI:10.15251/CL.2025.221.11

    Abstract As a potential substitute for antibiotics, cadmium sulfide and zinc oxide nano-particles (CdS and ZnO NPs) were created using laser ablation and a straightforward chemical process, respectively. Target of cadmium sulfide, deionized water, zinc nitrate, and sodium hydroxide were used as precursors. Different characterization techniques were used to characterize the CdS and ZnO NPs. X-ray diffraction was used to confirm that the CdS and ZnO had polycrystalline structures with average crystalline sizes of 54.16 nm and 29.23 nm, respectively. The ZnO particles were densely packed 2D curved nanopetals with a diameter of 51.65 nm, whereas… More >

  • Open Access

    ARTICLE

    Preparation and characterization of CuAlXSn1-XS2 thin films prepared by electron beam deposition system

    A. S. Alqarnia,, S. N. Alamrib,

    Chalcogenide Letters, Vol.22, No.5, pp. 493-506, 2025, DOI:10.15251/CL.2025.225.493

    Abstract Abundant and environmentally friendly solar cells materials Cu2AlSnS4 (CATS) thin film successively prepared by electron beam deposition system. The impact of various deposition times and post-annealing at 450 °C under nitrogen gas atmosphere on the structures, morphologies, and spectroscopic characteristics of the obtained CATS films were investigated. Both deposition time variation and annealing process were found to significantly affect the crystallinity, bonding vibration, surface morphology, energy band gaps, and Urbach energy of the CATS films. EDX spectra of the films disclosed the existence of all constituents’ elements. XRD analysis of the post-annealed films verified their multiple More >

  • Open Access

    ARTICLE

    Synergistic Regulation of Light Intensity and Calcium Nutrition in PFAL-Grown Lettuce by Optimizing Morphogenesis and Nutrient Homeostasis

    Jie Jin1, Tianci Wang1, Yaning Wang1, Jingqi Yao2, Jinxiu Song1,*

    Phyton-International Journal of Experimental Botany, Vol.94, No.11, pp. 3611-3632, 2025, DOI:10.32604/phyton.2025.070680 - 01 December 2025

    Abstract In plant factory with artificial lighting, precise regulation of environmental and nutritional factors is essential to optimize both growth and quality of leafy vegetables. This study systematically evaluated the combined effects of light intensity (150, 200, 250 μmol/(m2·s)) and calcium supply in the nutrient solution (0.5, 1.0, 1.5 mmol/L) on lettuce morphology, photosynthesis, quality indices, and tipburn incidence. Elevating light from 150 to 200 μmol/(m2·s) significantly enhanced leaf number, area, photosynthetic rate, biomass, and foliar calcium. These gains plateaued at 250 μmol/(m2·s), where tipburn incidence surged to 76.5%. Photosynthetic pigments progressively rose with light intensity. Calcium supply… More >

  • Open Access

    ARTICLE

    Dynamic Response Research of Dangerous Rockfall Impact Protection Structures

    Huaiqin Liu1, Meng Li1, Jianwen Shao2, Weishen Zhang1, Qifan Yang1, Yutong Li1, Tian Su1,3,*, Xuefeng Mei4

    Structural Durability & Health Monitoring, Vol.19, No.6, pp. 1563-1588, 2025, DOI:10.32604/sdhm.2025.073009 - 17 November 2025

    Abstract Rock collapse is a significant geological disaster that poses a serious threat to life and property in mountainous regions worldwide. Investigating the response of protective structures to rockfall impacts can provide valuable references for the design and placement of such structures. In this study, RocPro3D and ABAQUS were employed to comprehensively analyze rockfall movement trajectories and the structural response upon impact. The results indicate that when the impact velocity of rockfall at the protective structure reaches 20–30 m/sec, the corresponding bounce height ranges from 5 to 8 m, and most rockfall accumulates at the slope More > Graphic Abstract

    Dynamic Response Research of Dangerous Rockfall Impact Protection Structures

  • Open Access

    ARTICLE

    Multi-Environment Evaluation of Soybean Genotypes for Yield, Stability, and Trait Associations in Croatia

    Ivica Delic1, Goran Jukic2, Ivan Varnica2, Valentina Spanic3,*

    Phyton-International Journal of Experimental Botany, Vol.94, No.10, pp. 3189-3203, 2025, DOI:10.32604/phyton.2025.070489 - 29 October 2025

    Abstract This study evaluated agro-morphological traits, grain quality traits, and phenotypic stability of nine soybean genotypes across four environments over two growing seasons (2022–2023). Traits such as days to flowering, days to maturity, and disease symptoms were monitored throughout the season. At maturity, parameters including grain yield, grain oil and protein content, 1000-seed weight, test weight, scores of lodgings, shattering, plant height, and first pod height were evaluated. In addition, 18 morphological traits were scored, of which eight were sufficiently variable for further analysis. In terms of environmental stability, genotypes 2 and 13 excelled, while genotypes… More >

  • Open Access

    ARTICLE

    Enhancing Mechanical Properties of Biobased Polyurethane Composites Using Birch Flour and Diatomite Fillers

    Dmitry S. Konovalov1, Natalia N. Saprykina2, Vjacheslav V. Zuev1,2,*

    Journal of Renewable Materials, Vol.13, No.10, pp. 2043-2058, 2025, DOI:10.32604/jrm.2025.02025-0079 - 22 October 2025

    Abstract In this study, the polyurethanes (PU) were synthesized from 4,4-methylene diphenyl diisocyanate and biobased ethoxylated castor oil or one mixture of ethoxylated and neat castor oil by direct mixing method. Utilization of ethoxylated castor oil increases the tensile strength of PU up to 2.75 times (from 3.2 to 8.8 MPa), compared to PU based on neat castor oil. The PU composites filled with birch flour, diatomite, and their mixture were prepared using a homemade dissolver with a cutter-shaped attachment at a speed of 1500 r min−1. The tensile strength of PU composites filled with birch flour… More > Graphic Abstract

    Enhancing Mechanical Properties of Biobased Polyurethane Composites Using Birch Flour and Diatomite Fillers

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