X. L. Guo^a, Y. F. Zhang^a,*, S. Y. Li^b, Q. Li^b, Q. Hao^c, X. Y. Ran^c, Y. M. Zhao^d

Chalcogenide Letters, Vol.22, No.4, pp. 313-330, 2025, DOI:10.15251/CL.2025.224.313

Abstract MoS₂ has excellent properties but low conductivity, limiting its use in supercapacitors. Carbon’s high conductivity and stability enhance MoS₂’s electrochemical performance and cycling stability. This study prepared MoS₂/C composites via a one-step hydrothermal method, exploring the effects of solvents and carbon content. Deionized water as a solvent resulted in composites with large specific surface areas and good electrochemical properties. Increasing carbon content improved electrochemical performance, peaking at a glucose content of 0.28 mmol, achieving a specific capacitance of 202.6 F/g. However, excessive carbon content led to decreased performance. More >

A. B. Rzayeva^1,2,*, F. E. Abbdullayeva¹, S. C. Imanova¹, S. H. Aliyeva^1,2, S. N. Yasinova^1,2

Chalcogenide Letters, Vol.22, No.11, pp. 965-970, 2025, DOI:10.15251/CL.2025.2211.965

Abstract Lead indium selenide (PbIn2Se₄) is a promising chalcogenide semiconductor for optoelectronic and energy applications. We report a hydrothermal synthesis route using ethylene glycol under moderate conditions (433– 453 K, 7–12 h), yielding up to 85–87%. The product crystallized into a cotton-like morphology composed of nanoand microparticles. Structural and compositional integrity were confirmed by chemical analysis, thermogravimetric analysis, and transmission electron microscopy. These results demonstrate that hydrothermal synthesis provides an efficient and controllable pathway to high-purity PbIn2Se₄, opening opportunities for its use in advanced functional devices. More >

R. Gayathri^a, S. Shanmugha Soundare^b, K. Haritha^a, S. Ariponnammal^a,*

Chalcogenide Letters, Vol.21, No.12, pp. 1001-1009, 2024, DOI:10.15251/CL.2024.2112.1001

Abstract SnSO₃/ZnSO₃ nanocomposite has been synthesized using the hydrothermal process. The complete formation of the SnSO₃/ZnSO₃ nanocomposite is confirmed by XRD and EDAX. It displays a fascinating rectangular bar shape. The measured particle size is 100.4 nm. It will be a promising option for optoelectronic devices. Energy gap of the SnSO₃/ZnSO₃ nanocomposite is 5.85 eV. The refractive index of the nanocomposite through its energy gap is found to be 1.883. The ultraviolet (~387.2 nm) area of the PL emission spectrum exhibits the strong efficient emission, while the green (~522.1 nm) region and the red (~789.4 nm) region show More >

Deni Fajar Fitriyana^1,2,*, Rifky Ismail^1,3,*, Athanasius Priharyoto Bayuseno¹, Januar Parlaungan Siregar^4,5, Tezara Cionita⁶

Journal of Renewable Materials, Vol.12, No.6, pp. 1145-1163, 2024, DOI:10.32604/jrm.2024.052165 - 02 August 2024

Abstract Hydroxyapatite (HA) is a bio ceramic commonly utilized in bone tissue engineering due to its bioactive and osteoconductive properties. Crab shells are usually disregarded as waste material despite their significant CaCO content, and have not been widely utilized in the synthesis of HA. This study aims to synthesize and analyze HA derived from crab shells using the hydrothermal method with different durations of holding time. This study utilized precipitated calcium carbonate (PCC) derived from crab shells. With a hydrothermal reactor set at 160°C and varying holding times of 14 (HA_14), 16 (HA_16), and 18 (HA_18)… More > Graphic Abstract

Zun Bi^1,2,3, Ke Jia^1,2,3, Yunfei Liu^1,2,3,*, Yinong Lyu^1,2,3,*

Journal of Renewable Materials, Vol.10, No.2, pp. 431-451, 2022, DOI:10.32604/jrm.2022.016735 - 30 August 2021

Abstract A series of uniform single-phase spherical BaWO₄: Dy³⁺, Tm³⁺, Eu³⁺ phosphors were prepared via a microwave hydrothermal method by using trisodium citrate dehydrate as surfactant. The phase structure, morphology and photoluminescence properties were measured by powder X-ray diffraction, scanning electron microscope and fluorescence spectrometer, respectively. The results show that uniform spherical microcrystals with diameters in the range of 2–4 μm are obtained. And the phase and morphology of samples are not significantly changed by doping rare earth (RE³⁺) ions. Under the excitation wavelength of 356 and 365 nm, the samples BaWO₄: 0.03Dy³⁺, yTm³⁺ can emit cold white light. In order… More >

Peng Liu, Bin Bai, Cui Wang, Yunan Chen, Zhiwei Ge, Wenwen Wei, Hui Jin^*

Journal of Renewable Materials, Vol.9, No.12, pp. 2159-2174, 2021, DOI:10.32604/jrm.2021.016166 - 22 June 2021

Abstract In this paper, a simple method to plate a hydrophobic coating on the inner surface of a small-scaled tube was proposed, where the coating consisted of carbon microspheres. Three common plastics polystyrene, polycarbonate and polyethylene were used as the feedstocks to be processed in supercritical water in a quartz tubular reactor. After reaction, the contact angle of droplet on the inner surface of the quartz tube was turned out to be over 100°, significantly larger than that of the blank tube 54°. When processing polystyrene in the 750C supercritical water for 10 min, the largest… More > Graphic Abstract