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    ARTICLE

    Preparation of Dicarboxyl Cellulose Nanocrystals from Agricultural Wastes by Sequential Periodate-Chlorite Oxidation

    Xiaozheng Sun*, Qiang He, Yu Yang

    Journal of Renewable Materials, Vol.8, No.4, pp. 447-460, 2020, DOI:10.32604/jrm.2020.09671 - 24 April 2020

    Abstract Agricultural waste straw is the renewable resource with the highest annual yield in the world. In value-added applications of agricultural waste, dicarboxyl cellulose nanocrystals (DCCs) are prepared from rice, wheat, and corn straw by sequential periodate-chlorite oxidation. In this study, DCCs from rice, wheat, and corn straw were characterized by transmission electron microscopy (TEM), Fourier transform infrared spectrometer, X-ray diffractometer (XRD), and thermal gravimetric analysis (TGA). The carboxyl content of the DCCs was also investigated. XRD results show that the crystallinity index decreased after sequential periodate-chlorite oxidation; however, the cellulose I structure was maintained. TEM… More >

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