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  • Open Access

    ARTICLE

    Preparation and characterization of CuAlXSn1-XS2 thin films prepared by electron beam deposition system

    A. S. Alqarnia,, S. N. Alamrib,

    Chalcogenide Letters, Vol.22, No.5, pp. 493-506, 2025, DOI:10.15251/CL.2025.225.493

    Abstract Abundant and environmentally friendly solar cells materials Cu2AlSnS4 (CATS) thin film successively prepared by electron beam deposition system. The impact of various deposition times and post-annealing at 450 °C under nitrogen gas atmosphere on the structures, morphologies, and spectroscopic characteristics of the obtained CATS films were investigated. Both deposition time variation and annealing process were found to significantly affect the crystallinity, bonding vibration, surface morphology, energy band gaps, and Urbach energy of the CATS films. EDX spectra of the films disclosed the existence of all constituents’ elements. XRD analysis of the post-annealed films verified their multiple More >

  • Open Access

    ARTICLE

    Fabrication and characterization of Se66S44-xAsx thin films chalcogenide

    D. M. A. Latiff, B. A. Ahmed, S. M. Ali, K. A. Jasim*

    Chalcogenide Letters, Vol.22, No.6, pp. 521-528, 2025, DOI:10.15251/CL.2025.226.521

    Abstract In this paper, the effect of sulfur substitution by arsenic on the structural, optical properties of thin films of the trivalent chalcogenide Se66S44-xAsx at different concentrations (where x = 0, 8, 16, and 24 at %) was studied. Thin films with a thickness of (300±10 nm) were prepared using thermal evaporation of bulk samples. Structural examinations were performed using XRD and AFM techniques. All the studied film samples were amorphous in structure and the intensity of the crystalline parts was high in the range of 10-40. Also, in Atomic Force Microscopy (AFM). It was found that… More >

  • Open Access

    ARTICLE

    Synthesis and characterization of Cd1-xPbxSe (0≤ x ≤1) thin films deposited by chemical bath for photovoltaic application

    D. A. Adu-Boadua, M. Paala, M. B. Mensahb, I. Nkrumaha,*, R. Y. Tamakloea, F. K. Amponga, R. K. Nkuma, F. Boakyea

    Chalcogenide Letters, Vol.22, No.7, pp. 603-614, 2025, DOI:10.15251/CL.2025.227.603

    Abstract Cd1-xPbxSe (0≤ x ≤ 1) thin films with values of x = 0, 0.2, 0.4, 0.5 and 1, have been deposited by chemical bath technique for photovoltaic application. The deposition temperature, time and pH of the reactive solutions were 80℃, 150 min and 11 respectively. The XRD results confirmed the polycrystalline nature of all the films. It also showed that all the films exist in face centered cubic structures. There were no pure phases of CdSe and PbSe identified in the XRD results of the ternary compounds. The average grain sizes determined for each sample were… More >

  • Open Access

    ARTICLE

    Synthesis, characterization of zirconium doped cobalt nanoparticles and study of their thermoelectric properties

    Y. Arooja, A. Farhanb, S. Maqsooda,c, A. Eruma, M. Ishaqd, S. Rafiquea, A. Khalidb, F. Wazahata, M. A. Qamare,*

    Chalcogenide Letters, Vol.22, No.8, pp. 707-717, 2025, DOI:10.15251/CL.2025.228.707

    Abstract Chemical co-precipitation synthesis was used to make pure and zirconium-doped cobalt sulfide (Co3S4) nanoparticles (NPs). Important characterizations such as FTIR, UV-VIS, Raman, PL, SEM, XRD, and four probe methods were used to examine the influence of the Zr (0%, 5%, 10%, 15%, and 20%) doping on optical, electrical, structural, and thermoelectric characteristics of Co3S4 NPs. X-ray diffraction and SEM examination verified the cubic structure and grain size of pure and Zr-doped Co3S4-NPs. The FTIR spectrum revealed the rotational and vibrational modes linked to the material's surface. The material is optimal for photocatalytic activity with a redshift More >

  • Open Access

    ARTICLE

    Fe-doped SnO2-SnS2/polypyrrole: an efficient photocatalyst for the degradation of organic pollutant in wastewater

    F. Khana, S. Noreena, M. S. Youssefb, A. Jilanic, H. T. Alib, G. Mustafad, M. Zahida,*

    Chalcogenide Letters, Vol.22, No.9, pp. 807-820, 2025, DOI:10.15251/CL.2025.229.807

    Abstract In this study Fe doped SnO2-SnS2 (FS) and Fe doped SnO2-SnS2-polypyrrole (FS-PPY) were synthesized and studied for the methylene blue (MB) egrdation under UV light. The morphological and structural characterizations were carried out by FTIR, SEM-EDX, XRD and XPS. It has been found that FS-PPy degrade methylene blue upto 98 % under optimized conditions as pH =3, dye concentration = 10 ppm, oxidant dose = 2 mM. The Langmuir-Hinshelwood kinetics model fitted well. The optimization was studied using response surface methodology. Scavengers study was carried out to find the active species. Reusability of photocatalyst was evaluated More >

  • Open Access

    ARTICLE

    Synthesis and Characterization of Cu2ZnSnS4 (CZTS) Thin Films for Gas Sensor Applications

    F. T. Ibrahim1,*, A. A. Qassim2, S. M. A. Al-Dujayli1

    Chalcogenide Letters, Vol.22, No.11, pp. 929-937, 2025, DOI:10.15251/CL.2025.2211.929

    Abstract This work, pulse laser deposition technique was employee to synthesize Cu2ZnSnS4 (CZTS) thin films with different lasing energy (500, 600, 700, 800, 900 mJ). Through using different characterization technique to study structural, optical and gas sensing properties. the use of X-ray diffraction, the samples have polycrystalline with cubic structure. The EDX examination showed that the sample contains a suitable amount of Zn, Sn, Cu, and S atoms to form CZTS. UV-VIS measurement indicates that the synthesis of thin films employing a lower laser energy result in a drop in deposit sample thickness, which in turn More >

  • Open Access

    ARTICLE

    Solid Model Generation and Shape Analysis of Human Crystalline Lens Using 3D Digitization and Scanning Techniques

    José Velázquez, Dolores Ojados, Adrián Semitiel, Francisco Cavas*

    CMES-Computer Modeling in Engineering & Sciences, Vol.145, No.2, pp. 1821-1837, 2025, DOI:10.32604/cmes.2025.071131 - 26 November 2025

    Abstract This research establishes a methodological framework for generating geometrically accurate 3D representations of human crystalline lenses through scanning technologies and digital reconstruction. Multiple scanning systems were evaluated to identify optimal approaches for point cloud processing and subsequent development of parameterized solid models, facilitating comprehensive morpho-geometric characterization. Experimental work was performed at the 3D Scanning Laboratory of SEDIC (Industrial Design and Scientific Calculation Service) at the Technical University of Cartagena, employing five distinct scanner types based on structured light, laser, and infrared technologies. Test specimens—including preliminary calibration using a lentil and biological analysis of a human… More >

  • Open Access

    ARTICLE

    Microwave-Assisted Synthesis, Characterization, and Performance Assessment of Lemongrass-Derived Activated Carbon for Removal of Fe and Mn from Acid Mine Drainage

    Lailan Ni`mah1,*, Sri Rachmania Juliastuti2, Mahfud Mahfud2

    Journal of Renewable Materials, Vol.13, No.11, pp. 2169-2190, 2025, DOI:10.32604/jrm.2025.02025-0044 - 24 November 2025

    Abstract This study evaluates the effectiveness of microwave technology in producing activated carbon from lemongrass waste, an underutilized agricultural byproduct. Microwave-assisted production offers faster heating, lower energy consumption, and better process control compared to conventional methods. It also enhances pore development, resulting in larger, cleaner, and more uniform pores, making the activated carbon more effective for adsorption. The microwave-assisted process significantly accelerates production, reducing the required time to just 10 min at a power of 400 W. Activated carbon derived from lemongrass waste at 400 W exhibits a water absorption capacity of 7.88%, ash content of… More > Graphic Abstract

    Microwave-Assisted Synthesis, Characterization, and Performance Assessment of Lemongrass-Derived Activated Carbon for Removal of Fe and Mn from Acid Mine Drainage

  • Open Access

    ARTICLE

    Genome-Wide Identification and Characterization of FAR1 in Phaseolus vulgaris under Salt and Drought Stress Conditions

    Abdil Hakan Eren*

    Phyton-International Journal of Experimental Botany, Vol.94, No.10, pp. 3085-3107, 2025, DOI:10.32604/phyton.2025.069506 - 29 October 2025

    Abstract The FAR1-related sequence (FAR1) gene family consists of transcription factors that originated from transposases and is crucial for light signaling and stress adaptation in plants. Despite the recognized importance of FAR1 genes in model organisms, their genomic architecture, structural variability, and expression patterns in Phaseolus vulgaris have yet to be investigated. This study offers the inaugural comprehensive genome-wide identification and characterization of the FAR1 gene family in P. vulgaris. A total of 27 PvulFAR1 genes were identified, and their chromosomal distribution, gene structures, conserved domains, and phylogenetic relationships were analyzed systematically. The promoter regions of these genes were discovered… More >

  • Open Access

    ARTICLE

    LiSBOA: Enhancing LiDAR-Based Wind Turbine Wake and Turbulence Characterization in Complex Terrain

    Ahmad S. Azzahrani*

    Energy Engineering, Vol.122, No.11, pp. 4703-4713, 2025, DOI:10.32604/ee.2025.067398 - 27 October 2025

    Abstract The Light Detection and Ranging (LiDAR) data analysis method has emerged as a powerful and versatile tool for characterizing atmospheric conditions and modeling light propagation through various media. In the context of renewable energy, particularly wind energy, LiDAR is increasingly utilized to analyze wind flow, turbine wake effects, and turbulence in complex terrains. This study focuses on advancing LiDAR data interpretation through the development and application of the LiDAR Statistical Barnes Objective Analysis (LiSBOA) method. LiSBOA enhances the capacity of scanning LiDAR systems by enabling more precise optimization of scan configurations and improving the retrieval… More >

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