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  • Open Access

    PROCEEDINGS

    Peeling Induced Defects Investigation of Hydroxyapatite/Polymer Porous Structures Fabricated by Vat Photopolymerization

    Haowen Liang1, Jiaming Bai1,*

    The International Conference on Computational & Experimental Engineering and Sciences, Vol.30, No.2, pp. 1-1, 2024, DOI:10.32604/icces.2024.012563

    Abstract Defects are pivotal in influencing the mechanical performance of the hydroxyapatite (HAp) porous structure. In vat photopolymerization (VP) fabrication, directly peeling HAp/polymer green structure from the platform is an efficient approach but often introduces defects, compromising the mechanical performance of sintered HAp scaffolds. The peeling process is a physical phenomenon where the photocured HAp/polymer green structure exhibits resistance against applied peeling forces, which is influenced by its modulus and toughness. In this study, the peeling behavior of cubic-pore HAp (CP-HAp) green structures with varying levels of modulus and toughness was investigated in detail. The characterization… More >

  • Open Access

    ARTICLE

    Characterization of Hydroxyapatite Extracted from Crab Shell Using the Hydrothermal Method with Varying Holding Times

    Deni Fajar Fitriyana1,2,*, Rifky Ismail1,3,*, Athanasius Priharyoto Bayuseno1, Januar Parlaungan Siregar4,5, Tezara Cionita6

    Journal of Renewable Materials, Vol.12, No.6, pp. 1145-1163, 2024, DOI:10.32604/jrm.2024.052165 - 02 August 2024

    Abstract Hydroxyapatite (HA) is a bio ceramic commonly utilized in bone tissue engineering due to its bioactive and osteoconductive properties. Crab shells are usually disregarded as waste material despite their significant CaCO content, and have not been widely utilized in the synthesis of HA. This study aims to synthesize and analyze HA derived from crab shells using the hydrothermal method with different durations of holding time. This study utilized precipitated calcium carbonate (PCC) derived from crab shells. With a hydrothermal reactor set at 160°C and varying holding times of 14 (HA_14), 16 (HA_16), and 18 (HA_18)… More > Graphic Abstract

    Characterization of Hydroxyapatite Extracted from Crab Shell Using the Hydrothermal Method with Varying Holding Times

  • Open Access

    ARTICLE

    Investigation of the Nd-Ce-Mg-Zn/Substituted Hydroxyapatite Effect on Biological Properties and Osteosarcoma Cells

    Suha Q. AL-Shahrabalee*, Hussein Alaa Jaber

    Journal of Renewable Materials, Vol.11, No.3, pp. 1485-1498, 2023, DOI:10.32604/jrm.2023.025011 - 31 October 2022

    Abstract Cancerous diseases and diseases resulting from bacteria and fungi are some of the pressures that humans face. Therefore, the development of biomaterials that are resistant to cancerous diseases, bacteria, and fungi has become one of the requirements of the medical field to extend the life of the biomaterial and fight pathogens after implanting these materials inside the human body. One of the important biomaterials used in the field of orthopedics is hydroxyapatite. In this research, Nano substituted hydroxyapatite was prepared by the wet precipitation method, including replacing 5% of the calcium ions with neodymium, cerium, More > Graphic Abstract

    Investigation of the Nd-Ce-Mg-Zn/Substituted Hydroxyapatite Effect on Biological Properties and Osteosarcoma Cells

  • Open Access

    ARTICLE

    Agro-Industrial Waste as a Source of Raw Material: Eggshell and Ash of Agave salmiana Useful for the Synthesis of Hydroxyapatite

    Nora Elizondo-Villarreal1,*, Luz H. Verástegui-Dominguez1, Jose J. Quijano-Briones1, Francisco J. Vázquez-Rodríguez2, Eden Rodríguez-Castellanos3, Enrique López-Cuellar3, Ernesto Torres-Lopez1, Victor M. Castaño-Meneses4,*

    Journal of Renewable Materials, Vol.10, No.12, pp. 3559-3572, 2022, DOI:10.32604/jrm.2022.021945 - 14 July 2022

    Abstract

    Agave salmiana ash and poultry eggshell powder as CaO sources were used for obtaining nanostructured hydroxyapatite (HAP). The synthesis was carried out by the Green Chemistry Hydrothermal Biosynthesis at 180°C with a pH of 5, by reacting CaO from Agave Salmiana ash and Eggshell powder, with dibasic calcium phosphate (CaHPO4•2H2O) in an aqueous solution, with Aloe barbadensis extract. The product was characterized by X-ray diffraction, Fourier-transform infrared spectroscopy (FT-IR), Scanning Electron Microscopy (SEM), and Transmission Electron Microscopy (TEM). The size and shape of the hydroxyapatite particles changed dramatically in the presence of Aloe barbadensis. Large crystals of Hydroxyapatite were observed

    More > Graphic Abstract

    Agro-Industrial Waste as a Source of Raw Material: Eggshell and Ash of <i>Agave salmiana</i> Useful for the Synthesis of Hydroxyapatite

  • Open Access

    ARTICLE

    Mechanical and histological properties of an electrospun scaffold with a modified surface by plasma polymerization implanted in an in vivo model

    MARÍA G. FLORES-SÁNCHEZ1,*, ROBERTO OLAYO2, J. MORALES-CORONA2, ATLÁNTIDA M. RAYA-RIVERA3, DIEGO R. ESQUILIANO-RENDÓN3

    BIOCELL, Vol.46, No.3, pp. 829-836, 2022, DOI:10.32604/biocell.2022.016988 - 18 November 2021

    Abstract This article presents the construction of scaffolds composed of polylactic acid (PLA) with different concentrations of hydroxyapatite (HA) by electrospinning, which were superficially modified with polypyrrole (PPy/I) by plasma polymerization. A preliminary study was conducted of the biological and mechanical behavior of the scaffolds when they were implanted in the back of rabbits for 30 days; bone cells differentiated from mesenchymal stem cells (MSCs) were used. The bone cell and scaffold structures were characterized by histological, immunohistochemical, and mechanical stress tests. Hematoxylin–eosin staining showed good tissue conformation. The immunohistochemical tests highlighted the presence of the More >

  • Open Access

    ARTICLE

    Valorization of a Good Bioceramic from Moroccan Waste Fish Bone by a Heat Treatment Method

    Kaoutar Kara1,*, Fatiha Ouanji2, El Mostapha LOTFI1, Mohammed El Mahi1, Mohamed Kacimi2

    Journal of Renewable Materials, Vol.7, No.1, pp. 1-7, 2019, DOI:10.32604/jrm.2019.00016

    Abstract A tricalcium phosphate (TCP) material was produced from sardine and mackerel waste using a heat treatment method after a Soxhlet extraction to obtain the non-soluble portion of fish waste. The bones were annealed at temperatures between 400°C and 1200°C. The thermal analysis (TG-DTA) was carried out to investigate the thermal stability of TCP and to confirm the removal of organic matter from the raw fish. The calcined bones were characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), and field emission scanning electron microscopy (FE-SEM). The calcium to phosphorous weight ratio was determined by More >

  • Open Access

    ARTICLE

    Studies on Bone-Derived Calcium Phosphate Materials

    Agnieszka Sobczak-Kupiec1, Klaudia Pluta1, Dagmara Malina1*, Bożena Tyliszczak2

    Journal of Renewable Materials, Vol.5, No.3-4, pp. 180-188, 2017, DOI:10.7569/JRM.2017.634106

    Abstract In recent years, the development of composite biomaterials has been the subject of very intensive research. The elaboration of technology for manufacturing new biomaterials will allow their practical implementation and adaptation to changing market needs. One of the key components in the developed composite materials will be natural origin hydroxyapatite (HAp) and tricalcium phosphate (TCP) obtained from bone products. In this study, preparation and detailed characterization of bone-derived calcium phosphates as a component of biomaterial composites is proposed. This novel method of obtaining hydroxyapatite for biomedical applications allows the obtainment of a material with expected More >

  • Open Access

    ARTICLE

    3D Bio-Plotted Composite Scaffold Made of Collagen Treated Hydroxyapatite-Tricalciumphosphate for Rabbit Tibia Bone Regeneration

    Pranav S. Sapkal1*, Abhaykumar M. Kuthe1, Divya Ganapathy2, Shantanu C. Mathankar3, Sudhanshu Kuthe4

    Molecular & Cellular Biomechanics, Vol.13, No.2, pp. 115-136, 2016, DOI:10.3970/mcb.2016.013.131

    Abstract Biphasic calcium phosphate scaffolds with 20/80 HA/TCP ratio were fabricated using the 3D-Bioplotting system to heal critical size defects in rabbit tibia bone. Four different architectures were printed in a layer by layer fashion with lay down patterns viz. (a) 0°– 90°, (b) 0°– 45°– 90°– 135°, (c) 0°–108°– 216° and (d) 0°– 60°– 120°. After high-temperature sintering scaffolds were coated with collagen and were further characterized by (FTIR) Fourier Transform Infrared Spectroscopy, (SEM) Scanning Electron Microscopy, (XRD) X-Ray diffraction, Porosity analysis and Mechanical testing. Scaffold samples were tested for its ability to induce cytotoxicity… More >

  • Open Access

    ARTICLE

    AFM and Nanoindentation Studies of Bone Nodules on Chitosan-Polygalacturonic Acid-Hydroxyapatite Nanocomposites

    R. Khanna1,2, D. R. Katti1, K. S. Katti1

    CMES-Computer Modeling in Engineering & Sciences, Vol.87, No.6, pp. 530-556, 2012, DOI:10.3970/cmes.2012.087.530

    Abstract Here we report a new in situ nanoindentation technique developed to evaluate the composite mechanical behavior of cell-biomaterial construct under physiological conditions over the time scale of bone nodule generation. Using this technique, mechanical behavior of osteoblast cell-substrate interfaces on tissue engineered materials (chitosan-polygalacturonic acid-nanohydroxyapatite (CPH) films) is investigated. Mechanical behavior of cells in the elastic regime over the time scale of cell adhesion (1 day), proliferation (4 days), development (8 days) and maturation (22 days) of bone nodules is evaluated. Our results indicate that the elastic properties of flat cells are higher (indicating stiffer… More >

  • Open Access

    ARTICLE

    Wet-chemical Synthesis and Magnetic Property Studies of Fe(III) Ion Substituted Hydroxyapatite

    K. H. Prakash1, R. Kumar2, C. P. Ooi1, T. Sritharan3, P. Cheang1, K. A. Khor4

    Molecular & Cellular Biomechanics, Vol.3, No.4, pp. 177-178, 2006, DOI:10.32604/mcb.2006.003.177

    Abstract This article has no abstract. More >

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