Zhi Xu, Yoshio Bando, Lei Liu, Wenlong Wang, Xuedong Bai, Dmitri Golberg
The International Conference on Computational & Experimental Engineering and Sciences, Vol.17, No.2, pp. 41-42, 2011, DOI:10.3970/icces.2011.017.041
Abstract A specially designed suspended graphene oxide (GO) device has been fabricated and investigated in a transmission electron microscope (TEM)-scanning tunneling microscopy (STM) based setup. The detailed study of step-by-step slow reduction of an individual GO sheet under current flow and thereby Joule heating, while in-parallel performing conductivity measurements, atomic structure imaging, chemical composition, and bonding alternations tracing have been performed. As monitored by electron energy core loss spectroscopy, the oxygen content is tuned from that peculiar to a pristine GO, i.e. 23.8 at.%, to oxygen-free pure graphene. Six orders of magnitude conductance rise is achieved… More >