Open Access
ARTICLE
The Accelerated Thermo-Oxidative Aging Characteristics of Wood Fiber/Polycaprolactone Composite: Effect of Temperature, Humidity and Time
Shuang Si, Qian Tang, Xingong Li*
Central South University of Forestry and Technology, Changsha, 410004, China
* Corresponding Author: Xingong Li. Email:
Journal of Renewable Materials 2021, 9(12), 2209-2222. https://doi.org/10.32604/jrm.2021.015506
Received 23 December 2020; Accepted 25 February 2021; Issue published 22 June 2021
Abstract
This study investigated the characteristics of wood fiber/polycaprolactone composite after an artificial accelerated
thermo-oxidative aging treatment. The effect of time, temperature and humidity during the treatment on their
mechanical, chemical and morphology properties were evaluated. The composite was prepared from melted wood
fibers and modified polycaprolactone by a molding process. A temperature and humidity controllable test chamber was used for the thermo-oxidative aging of the composite. The thermo-oxidative aging caused surface of the
composite to be much more rougher and even a few cracks and holes appeared on it. According to the spectra of
Fourier Transform Infrared (FTIR) and Gel Permeation Chromatography (GPC), C=O in the molecular chain of
polycaprolactone was hydrolyzed and C–O was broken after the aging treatment, which resulted in a reduction in
average molecular weight of the composite. Moreover, results showed that the mechanical strength decreased a lot
with the increase in time, temperature and humidity, and the effect of temperature and humidity was more significant compared with that of time. Controlling the temperature and humidity during thermo-oxidative aging
treatment could accelerate the aging of composite, which provided a quick and effective method for evaluating
the aging resistance of the composite.
Graphical Abstract
Keywords
Cite This Article
APA Style
Si, S., Tang, Q., Li, X. (2021). The accelerated thermo-oxidative aging characteristics of wood fiber/polycaprolactone composite: effect of temperature, humidity and time. Journal of Renewable Materials, 9(12), 2209-2222. https://doi.org/10.32604/jrm.2021.015506
Vancouver Style
Si S, Tang Q, Li X. The accelerated thermo-oxidative aging characteristics of wood fiber/polycaprolactone composite: effect of temperature, humidity and time. J Renew Mater. 2021;9(12):2209-2222 https://doi.org/10.32604/jrm.2021.015506
IEEE Style
S. Si, Q. Tang, and X. Li "The Accelerated Thermo-Oxidative Aging Characteristics of Wood Fiber/Polycaprolactone Composite: Effect of Temperature, Humidity and Time," J. Renew. Mater., vol. 9, no. 12, pp. 2209-2222. 2021. https://doi.org/10.32604/jrm.2021.015506