Liquefaction of Kraft Lignin at Atmospheric Pressure
Silvia Helena Fuentes da Silva1, Patricia Soares Bilhalva dos Santos2, Darci Alberto Gatto3, Maria Angeles Andres1, Itziar Egüés1,*
Journal of Renewable Materials, Vol.7, No.6, pp. 527-534, 2019, DOI:10.32604/jrm.2019.04291
Abstract Kraft lignin was liquefied using polyethylene glycol #400 (PEG) and glycerol (G) in a weight ratio of 80/20 (w/w) and sulphuric acid (SA) as catalyst under atmospheric pressure at 160ºC. The three independent variables: reaction time (60, 80 and 100 min), percentage of lignin (15, 20 and 25%, w/w), and catalyst concentration (0, 3 and 6%, w/w), were varied resulting in 27 experimental runs. The effect of these reaction conditions on the properties of the polyols was evaluated. The statistical analysis showed that only “the percentage of lignin” did not influence the properties of the More >