Physicochemical Characterization and Antimicrobial Properties of Inulin Acetate Obtained by Microwave-Assisted Synthesis
Nadezhda Petkova, Radka Arabadzhieva, Dragomir Vassilev, Gergana Gencheva, Yulian Tumbarski, Tsveteslava Ignatova-Ivanova, Sevginar Ibryamova, Mina Todorova, Milena Koleva, Panteley Denev
Journal of Renewable Materials, Vol.8, No.4, pp. 365-381, 2020, DOI:10.32604/jrm.2020.09292
(This article belongs to the Special Issue:
The 10th Conference on Green Chemistry and Nanotechnologies in Polymeric Materials (GCNPM 2019))
Abstract Microwave-assisted irradiation was performed for esterification of chicory inulin with high degree of polymerization with acetic anhydride without a solvent only with a catalyst. The resulting esters were characterized by melting point,
hydrophilic-lipophilic balance, thin-layer chromatography, ultraviolet spectroscopy, Fourier transform infrared spectroscopy (FTIR) and nuclear magnetic resonance (NMR) spectroscopy. Inulin acetate demonstrated a high degree of
acetylation (2.5–3.0) and presented a white, water-insoluble substance with bitter
taste. The FTIR and NMR spectra confirmed esterification and demonstrated the
incorporation of hydrophobic residue to the water soluble inulin backbone. Swelling capacity, water holding, oil-holding capacities, the foamability,…
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